GCMS results log, sample AD26983, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26983.D Vial: 25 Acq On 7 Dec 2001 7:59 am Operator: GALOS Sample g c/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.04 0.54 ng/uL 195594 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane/ methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohex. ne, methyl- 98 C7H14 000108-87-2 95 4 Cyclohex ne, methyl- 98 C7H14 _______ 000108-87-2 64 'Abundance / Scan 21 (5.037 min): 26983. D (-) m/ z .83.05 100.00% 55 83

41 5000 98 69 r 1' ■ 1 ■ ’1' i • ■ • • i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 ■ i " ■ ■ i " ■' r 1 +—514 +rr .. Illi....... I + 94 i1" i TTTTTit m/z ,55.10 99.84% miz-s 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- I 55 83 I I

5000 98 AA ■ ■ i. ■ i.. I' ’'' I

42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 41.00 70 m/ z 51.60%

m/z-> Abundance

5000 ' ■ i ■''' i1

27 ’ l1M ■ i * 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #1326: Cyclohexane, methyl-

42 ' i1

55 4-rr 661 -rp-rr

69 TI‘

83 +ror

98 TTTTT I I . I ... I I I I I I I . 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z ANL 98.05 44.74% nrm

i •' I • ‘ " I " ’' I' 11" 11 TT '■ i*'1' r ■ >■ i"r " ' i • ■"i" " m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 I80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- / ______________ T‘ '1 i'b ’ H •'''I " ''i’ • ■' I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ z 42.00 33.79%

_AN 5000 98 42 69 27

m/z-> ml 20 25 ' i " " I ■ " 11' 30 35 40 " i " ■' i " 45 50 55 60 ... —... T 65 70 75 80 +85 90 95 100 105 11'1 'I 4.90 5.00 5.10 5.20 5.30 5.40 5.50 TTfITAT

26983.D NP112701.M Tue Dec 11 14:49:33 2001 Page 1

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