GCMS results log, sample AD26992, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26992.D Vial: 18 Acq On 7 Dec 2001 1:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.51 ng/uL 207621 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexanes methyl- 98 C7H14 000108-87-2 97 2 Cy c l ohexane , methyl- 98 C7H14 000108-87-2 96 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 4 Cy c l ohexane , methyl- 98 C7H14 000108-87-2 60 Abundance Scan 23 (5.049 min): 26992.D (-) m/ z 83.05 100.00% 55 83 41 5000 98 69 ... —........ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 51. - t HT ' i'11' 11 +1 Tp-rrrp-r m/ Z 55.10 99.87% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83 i i I - —A AAmp 5000 98 42 I 4.90 5.00 5.10 5.20 5 0 5.40 5.50 27 70 m/z 41.10 56.80% j m/z-> .Abundance 20

5000- ■ i " ■ ■ r 25

27 ' r ''' i " ' ■ i' • i • ■ ■ ■ i• TTI 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63235; Cyclohexane, methyl- 55

42 83 661 TTT

69 I'11' I i •" • i1 • " i +r

98 A MAAA 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 98.15 46.55%

■I•’"I"'•| ■ ITTTTTTTTTTTTTTTTTTTTTT । ।. .i । ।. r. p T’TTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- — ......... — 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z .42.05 35.06% 5000 98 42

m/z-> -rp-rrrp- 20 25 27

I’’ ’, TTT TIp m 69

111" • i ■ ■ • ■ i ■ ■ ■ i " '1 r ■ 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 IW r AA 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26992.D NP112701.M Tue Dec 11 14:55:14 2001 Page 1

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