GCMS results log, sample AD26991, Dec 11 2001

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Library Search Compound Report

■ Data File C:\HPCHEM\l\DATA\DEC0601\26991.D Vial: 17 Acq On 7 Dec 2001 12:43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

5.03 0.52 ng/uL 168172 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 78 ■Abundance Scan 21 (5.032 min): 26991.D (-) m/ z 83.05 100.00% 56 83

5000- 41 98 69 TT 4.90 5.00 5.10 5.20 5.30 5.40 5.50

miz-> +51+ 1pr .. ..... U 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 11 ■ ■ ■ ■ । • 94.29% Abundance #63235: Cyclohexane, methyl- 55 83

5000 98 11'1 ■' 11 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 69 m/z 41.10 45.76%

U 27

m/z-> L . .... —m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 " i " '' i1' TT’ T ITTT

Abundance #63236: Cyclohexane, methyl- 55 83

4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- 98 m/z 98.05 45.42% 27 42 70 66 ■ | l i l • |« l ! ( | ! I i I | ■ i" " r " 1 r' " i "'11' r "11 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- i ’ ■ ’' i I’ 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42.00 34.55% 5000

m/z--> 27

TTT’t’IT Th- i" " । 42

TTTTTT +TT -H- 69 -PTPT 11 ■ "111 ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 98

, LA . TI‘ 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26991 .D NP112701.M Tue Dec 11 14:54:20 2001 Page 1

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