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GCMS analysis report for sample AD26472, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26472 noting other unknown compounds.

NYC-WTC_000031611–000031623

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26471.D Vial: 11 Acq On : 30 Nov 2001 9:19 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.05 0.47 ng/uL 216658 1,4-Dichlorobenzene-d4 11.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 4 Cyclohexane, methyl-__________ 98 C7H14 000108-87-2 78 Abundance 7 Scan 22 (5.046 min): 26471 .D (-) m/z 83.05 100.00% ] 55 83

41 98 5000 69 I ■1" I “ i “ ■' i 1’’ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 51 mm mm HH —m1 - m/z 55.10 96.34% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83

5000 98 —P n 11 TmTu TT 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 41.00 51.36%

XN 69 27 * - ■ H m Hmmm t mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 8? 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 45.48% 42 27 70 m mmmmm m ' Hfl ■ m ’ Hmmm Hmmm mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- ' 11"111"11"1TTPTTTT 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z42.00

N 32.34%

5000 98 42 27 69 11 111 " — ——— rrrrp- - - HH - mm H TAA miz—> 20 25 3035404550556065 70 75 80859095 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26471.D NP112701.M Tue Dec 04 10:44:25 2001 Page 1

NYC-WTC_000031619

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NYC-WTC_000031619Source: NYC Law Department, mirrored locally

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