GCMS analysis results sample AD26472, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26472.D vial: 10 Acq On : 30 Nov 2001 8:25 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.06 0.45 ng/uL 216937 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohex he, methyl- 98 C7H14 000108-87-2 95 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 91 4 Cyclohexane, methyl- 98 C7H14 000108-87-2 78 Abundance Scan 23 (5.056 min): 26472.D (-) m/z 83.05 100.00% 55 8ts

5000 41 98

70 •' i" “ i “ “ i “ “ i"

miz-> —+l+ fpu TTTTTTT n 77 Hm Hmm m/z55.05 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50 90.99% Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 -Mmfmftmm 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/z 98.05 49.74%

miz-> tt j it 14 r 4 l J lit* IT 1 tip i»| rm 11111 20253035404550556065 70 75 80859095 100 105 —fl-m Hmmmp +tt I I I I I I TTTTT

Abundance #1326: Cyclohexane, methyl- 83 55 11■111111•i “1■i ■ “ ■ i“ ■11 *“ ■ i ■'1 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 41.00 48.13% 42 27 69

111’11111 T’T—11—ar Trnrrrj-rrrr tmmme TT——gu11 mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- — 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 34.75%

5000 98 42 69 27 4pmmp . . 14 . . > j < > 1 > l < . ..!. t .. 1. ■ ■' 'i” ■11‘ 1AA4,A m/z—> 20253035404550556065 70 75 80859095 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26472.D NP112701.M Tue Dec 04 10:44:44 2001 Page 1

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