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GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032389–000032399

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26985.D Vial: 31 Acq On 7 Dec 2001 2:24 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.03 0.44 ng/uL 151907 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 94 'Abundance Scan 20 (5.028 min): 26985.D (-) m/ Z 83.05 100.00%l 55 83

5000 41 98 69 ) T TT I' ■ ' • I' 4.90 5.00 5.10 5.20 5.30 5.40 1 I m/z—> ' i ■'" i " ■ ■ i ■ 20 25 30 35 --PH i 51, 40 45 m. - - —I 50 55 60 65 70 75 80 85 90 1Te 95 100 105 m/ z 55.10 92.14% Abundance #1326: Cyclohexane, methyl- 55 83

5000 98 ----- 42 4.90 5.00 5.10 5.20 5.30 5.40 27 69 m/z .41.05 43.26% i

W i . I! -P+ ,, ।, '111' ’ 11 ' r ' ■' i " '' i' ‘r " ' i■ ' r " ■ r ■ m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83

4.90 5.00 5.10 5.20 5.30 5.40 | 5000- 98 m/z 98.15 41.17% 42 69 27 ' i'1' ‘ r "' i' "' i'"' i' " ' r "' i ■ ■ " i11'' r " ' i ■ " ' i'1" i'' ■ ‘ i ■ " ' i1 ■'' i'' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- I'' •' I' •'' I' 55 83 4.90 5.00 5.1G 5.20 5.30 5.40 m/ Z 42.10 29.21%

UA 5000 98 42 27 70

11' " 111 III r ■ " r 1' [ " " I " 11' ‘ ' i' +1TT Tp-rrrp-r l. ,, MAA J, AM , ,, ,, TITT m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 | 4.90 5.00 5.10 5.20 5.30 5.40

26985.D NP112701.M Tue Dec 11 14:50:24 2001 Page 1

NYC-WTC_000032397

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NYC-WTC_000032397Source: NYC Law Department, mirrored locally

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