GCMS results log, sample AD27011, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\27011.D Vial: 19 Acq On 7 Dec 2001 2:32 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.52 ng/uL 201416 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

lCyclohexane,/methyl - 98 C7H14 000108-87-2 97 2Cyclohexane, methyl- 98 C7H14 000108-87-2 91 3Cyclohexane, methyl- 98 C7H14 000108-87-2 86 43-Penten/2-one, 4-methyl- 98 C6H10O 000141-79-7 50 Abundance .■ Scan 23 (5.050 min): 27011 .D (-) m/z 83.05 100.00% 55 83

41 98 5000 69 i' ■ ■ ■ i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 I miz-> 20 ■ i'' ■' i " 11111'111 25 30 35 40 +51+ —mH 45 50 55 60 65 70 75 80 — — 85 90 T‘ "IT 95 100 105 m/z 55.10 89.22% Abundance #1326: Cyclohexane, methyl- 83 55

5000- 42 98 Ae r••*i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 69 m/z 41.05 49.82% 1 'I T’EITT TTTTTTTTTTTTTTTITT 11gr 1’’’ 11" " I " m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance (¥63236: Cyclohexane, methyl- I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 45.38% 42 27 70 66 PTTTTrr TTTTT t TTT 11 > I, >.. ।11 >, < 11 ■... ।.।,।, 'T'''11' T’’ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63234: Cyclohexane, methyl- T’TTTT T’T 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42.00 31.09%

m/z-> 5000-

mm 27 42

-PTT rrr +r TTT ' ■ I'" ' I " 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 AAAM 69

' I " ' ■ I' 4.90 5.00 5.10 5.20 5.30 5.40 5.50 98

i ■ ‘1 ■ I A__ 27011.D NP112701.M Tue Dec 11 15:00:07 2001 Page 1

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