GCMS analysis results for sample AD26315, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26315 with unidentified compounds detected.

NYC-WTC_000031248–000031261

Folder label: “GCMS X 11/3/01 A 12/1/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV3 001\26315.D Vial: 24 Acq On 1 Dec 2001 9:07 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank: 2 R.T. EstConc Area Relative to ISTD R.T. 5.03 0.83 ng/uL 235001 1,4-Dichlorobenzene-d4 11.89 .Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclohexa: , methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 93 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 90 4 Cyclohexane, methyl-______ 98 C7H14 000108-87-2 72 Abundance Scan 21 (5.031 min): 26315.D (-) m/z 83.05 100.00% / 55 83

5000 41 98 69 l>' “ i■ । " i1 ■ “i■ " ■ i ■1111 ■

mfe-> ' ‘ i' ‘ ' i " " I''' ■ i' ■ ■ I —l+ ml — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 79 -rrprrrrjT 4.90 5.00 5.10 5.20 5.30 5.40 hmmpmpt Imn m/z ,55.10 97.95% Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 42 4.90 5.00 5.10 5.20 5.30 5.40 " ' ‘ 27 70 m/z 41.05 49.50%

miz-> -rrprrrrp- 1111117 1 • “ • I* TTp-rrrp-rTT Hr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 —fill.. m 111111111111 ■ ■ Ipumn

Abundance #63235: Cyclohexane, methyl- 55 83 TOTTTTTTTTTT TIm) 4.90 5.00 5.10 5.20 5.30 5.40 5000 98 m/z .98.05 43.13% 42 69 27 ■' i" mmm . ....... H ■|1 • • ■ | • r | " TTUgor m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- —। .. \i.............. । 11 11 । 11 11 11 i r-i |-i i 11 । i ■ 83 4.90 5.00 5.10 5.20 5.30 5.40 55 m/z 42.05 30.33% 5000 98 42 27 69

m/z—> " I''111' i‘ '11'''' I''' ‘ 20 25 3035404550 55 6065 70 75 80 85 90 95 100 105 mH m Ip 11" "i“" i" " । ।"1 ■ । “1111'111"1111 4.90 5.00 5.10 5.20 5.30 5.40

26315.D NP112701.M Tue Dec 04 10:11:44 2001 Page 1

NYC-WTC_000031256

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NYC-WTC_000031256Source: NYC Law Department, mirrored locally

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