GCMS analysis report for sample AD26433, Dec 2001

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Library Search Compound Report . Data File C:\HPCHEM\1\DATA\NOV3001\26433.D vial: 21 Acq On 1 Dec 2001 6:24 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.05 0.49 ng/uL 240118 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 4 Cyelohexane, methyl - 98 C7H14 000108-87-2 86 Abundance Scan 22 (5.047 min): 26433.D (-) m/z 83.05 100.00% 55 83

5000 41 98 69 4.90 5.00 5.10 5.20 5.30 5.40 5.50 ■■। । ।।■ 11 —5l Hmr f.. 74 —Pp m/z 55.10 90.37% mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 83 55

5000 98 am 1 4.90 5.00 5.10 5.20 5.30 5.40 5.50 42 69 m/z41.0 45.76% 27 mmmm "I " "I " 11 Hpur ■ > i««11|' । ■ 11 > ■ ।n। 1TTTT -t-p-rrrp-rrt mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83 i'''' i “ “ i" “ i T ToMffr 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 44.48% 42 27 70

■' i ■ i' ' ■ i1 ■ ■ ■ i'''' i' Irr ........................... . Ippr Imgun miz-> 20 25 3035404550556065 70 75 80859095 100 105 Abundance #1326: Cyclohexane, methyl- 55 83 A • i1 ‘111 “ “ i “ 1' i “ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42.05 31.14% 5000

m/z—> 27 42

’1’01107 ‘ ■ i ■ ■ ‘ ■ i'1'' i' 69 98

Hgar l....... pl { JTTI I|I> <IJ I■ 112310 20 25 30 35 40 45 50 55 60 85 70 75 80 85 90 95 100 105 AN. 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26433.D NP112701.M Tue Dec 04 15:08:12 2001 Page 1

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