GCMS analysis results for sample AD26321, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \HPCHEM\1 \DATA\NOV3 001\26321.D Vial: 31 Acq On 1 Dec 2001 3:30 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.04 0.81 ng/uL 245200 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexa: e, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexa e, methyl- 98 C7H14 000108-87-2 95 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 4 Furan,2,5-dihydro-2,5-dimethyl- 98 C6H10O 059242-27-2 53 Abundance Scan 22 (5,043 min): 26321.0 (-) m/z 83.05 100.00% 55 83

41 98 5000 69 — A— r m 4.90 5.00 5.10 5.20 5.30 5.40 5.50 51 Tm , TIT TIUT Tm TTI 65, । m/z 55.10 96.40% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 83 55

5000 98 111— ‘ mPm m r 4.90 5.00 5.10 5.20 5.30 5.40 5.50 42 69 m/z41.0 51.01% 27 mmm tm .J "1“ Ip mlz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83 i1 ’ ‘ 1— TTTTTTTTTT J. i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 45.66% 42 27 70

mz-> * • i • • • • I«•1 ■ 1 • Trp-rrrp-rrr '' i ■ ■ ■ ■ i ‘ +ll. m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 +pmppe IPpum

Abundance #1326: Cyclohexane, methyl- i"■*i■’111 “ ■11 ■ ■ ■ • i"1 ‘ i ■1141 “ 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z42.05 32.81% 5000 98 __ 42 27 69 - m/z—> H “I ‘ “ 1 1“ “l* 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 t । 13 > I | I I i i 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26321.D NP112701.M Tue Dec 04 10:13:27 2001 Page 1

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