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GCMS analysis results for sample AD26318, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26318 with unidentified compounds detected.

NYC-WTC_000031284–000031296

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\26318.D Vial: 28 Acq On 1 Dec 2001 12:46 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.04 0.47 ng/uL 226556 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohex , methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 4 Furan, 2,5-dihydro-2,5-dimethyl- 98 C6H10O 059242-27-2 53 Abundance Scan 21 (5.035 min): 26318.D (-) m/z 83.05 100.00% 55 83

5000 41 98

70 I’r i “ ' ■ i ■ • • ■ i “ ' ‘ i1 •'' i' 4.90 5.00 5.10 5.20 5.30 5.40 5.50 51 , , J 77 । 94 , m/z 55.10 86.56% TIOTTTTTm mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 AAmmntm —4.90 — 5.00 5.10 5.20 5.30 5.40 5.50 42 27 m/z 41.05 48.24%

AA 70

miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83 . 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 45.74% 42 69 27

mz-> mm m ■ tm+ ' m Im 11“1' i ■ ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 11

Abundance #1326: Cyclohexane, methyl- / 1’1211112111111’11’111101’11171 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z42.05 31.27%

5000

m/z—> 27 42

m mm m ' H+ ' m Hm H 69

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 98

ANl • ’ • • 1 • •«’ J ‘*11 * ‘111 ‘ 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26318.D NP112701.M Tue Dec 04 10:12:42 2001 Page 1

NYC-WTC_000031292

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NYC-WTC_000031292Source: NYC Law Department, mirrored locally

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