GCMS analysis report for sample AD26434, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26434.D Vial: 22 Acq On : 1 Dec 2001 7:18 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.05 0.46 ng/uL 222269 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual l Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl - 98 C7H14 000108-87-2 94 4 Furan, 2^5-dihydro-2,5-dimethyl- 98 C6H10O 059242-27-2 59 Abundance 7 Scan 23 (5.055 min): 26434.D (-) m/z 83.05 100.00% 1 55 8)3

41 98 5000 69 1’1’11 "1111111’11111117’271- 4.90 5.00 5.10 5.20 5.30 5.40 5.50 TTpr TTjs 1 111T r 1 JIJ I | 51, 65 77 H | J'l 11 | ITT TTprajent i ) i : | i It i j 1 | 11 M 11 j 111: |: ( f j: t : J j t i: 1 m/z 55.10 88.52% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 8?

5000 98 TIPTu 11’111411 4.90 5.00 5.10 5.20 5.30 5.40 5.50 42 27 70 m/z 41.05 48.51%

mz-> Abundance

5000 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63235: Cyclohexane, methyl-

42 55 83

98 AA_ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 98.05 48.21% 69 27 . mmmmm mm - t ' m Im H 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 miz—> Abundance #1326: Cyclohexane, methyl- 1’ “ 111" I i “i 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/ z 56.1 31.74%

5000 98 42 27 69 mH H m ' H+ mp t H To ।• •. • ।• 11“ •. । i mz--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26434.D NP112701.M Tue Dec 04 15:41:38 2001 Page 1

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