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GCMS Analysis Report for Sample AD26389, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.

NYC-WTC_000031473–000031490

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 Nov 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.04 0.49 ng/uL 208839 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexanes methyl- 98 C7H14 000108-87-2 94 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 91 4 Furan, 2,5-dihydro-2,5-dimethyl- 98 C6H10O 059242-27-2 59 Abundance 2 - Scan 22 (5.041 min): 26389.D (-) m/z 83.05 100.00% 55 83

41 5000 98

69 ...L............. —i •••■i' " ‘ i • ■ “ i “ i ■ " ■ i‘‘'i'■ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 ....... .. 511 ;... 1 ... 1.... . .. “ I “ " I' ‘" 11" ‘ I' “111'" I “ " 11'111111 ‘ 11 ‘ “ I ‘ “11" I ‘ l1" , I' ‘111" ‘ ‘ I" “ 1' “11'11' I"1 m/z 55.10 87.79% mlz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

U Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 T 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/z 41.05 56.47%

miz-> 1 ■ i ■ ■ ‘ ■ i1 ' ‘ I ■ ‘ ‘' i' • • ‘ i • Irr - 1 —Hmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83 1-1111111/11117110TT’t’T2’11T 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.15 49.24% 42 69 27

miz-> ’ 157111111117170112711 1’1’1111111 +TT-TT mHTTT —mp IImIpor 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z42.0 29.37% 5000 98 42 27 69

m/z—> ’II TTI ‘ 'I 'l“ “11 pur —mmmp -H 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TTTTTTTui 4.90 5.00 5.10 5,20 5.30 5.40 5.50

26389.D NP112701.M Tue Dec 04 10:41:03 2001 Page 1

NYC-WTC_000031481

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NYC-WTC_000031481Source: NYC Law Department, mirrored locally

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