GCMS Analysis Report for Sample AD26389, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 NOV 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Pentanol, 4-methyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.15 1.05 ng/uL 445903 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 25 2 l-Butanol / 74 C4H10O 000071-36-3 23 3 Oxirane, (1-methylethyl) - 86 C5H10O 001438-14-8 12 4 Cyclopropa: , (1-methylethyl)- 84 C6H12 003638-35-5 10 Abundance Scan 34 (5.151 min): 26389.D (-) m/z 41.10 100.00% 41 56 59

5000

45 71 • 1 । •FmTTTr TI . 5.00 5.20 5.40 5.60

miz-> । ■" ■ । • ■ ■11 “ “ । ■ 20 25 30 35 3440 .145 5050 5355 60opep । [ । ri1111 (। 67 65 70 75 80 85 90 95 m/z ' i “ ‘ ■ i • “ ■ i “ “ i'' " i !56.10 80.06% Abundance #63578:1-Pentanol, 4-methyl- 56 41 69 5000 =TTTETr 5.00 5.20 5.40 5.60 m/z 59.10 78.60%

miz-> 4 — ll 59 TImu Tmutma ।1 ■ “ । •1 ■ • ।1 ‘■■।■' “ । 84 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62584: 1-Butanol 41 56 • ■ । ■ • ■ ■ । 1 । • 1 • । ' 5.00 5.20 5.40 5.60 5000 m/z 43.10 66.21%

mz-> Abundance 1..,20.......... +53l —160— 45 .31 _______________________ 25 30 35 40 45 50 55

41 65 70 75 80 85 90 95 #721: Oxirane, (1-methylethyl)- 56 A 5.00 ‘ ' 5.20 ' ‘ 5.40 ' ' 5.60 m/z 42.10 62.98% 5000

27 —20....25I..... 37 N... 50531 , ■ i ■' ■ ■ i 71 85 TTTir m/z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 ' 5.40 5.60

26389.D NP112701.M Tue Dec 04 10:41:04 2001 Page 2

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