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GCMS analysis results for sample AD26828, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26828 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032182–000032201

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032191
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26828.D Vial: 12 Acq On 6 Dec 2001 8:12 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Pentanol, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.11 1.34ng/uL 334885 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 36 2 1-Butanol 74 C4H10O 000071-36-3 28 3 Cyc obutane 56 C4H8 000287-23-0 9 4 2-P tene, (E)- 56 C4H8 000624-64-6 9 Abundance Scan 30 (5.114 min): 26828.D (-) m/z 41 05 100.00% 41 56 59

5000-

71 TT 11 ■'' i' ■ " i IE‘‘I"TTTT 45 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z-> 15 20 25 30 35 4 49 53/ 40 45 50 55 60 65 70 I *1111 ■ । 67 | । r> ■ ■ • i • ■ ' • i ■ ■ - ■ i1 ■ ■ ■ ।• 75 80 85 90 m/z 56 10 83.18% Abundance #63578:1-Pentanol, 4-methyl- 56 41 69 5000 T| 11 11 111 M | Prrr ] TTpT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 59,10 70.93% 145 I | 59 84 11 I''' • I •''' I '111111111 h 1 ■ ■ -1 ■ • ■ ■ i ■' ■' TPBITT miz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ■Abundance #62584: 1-Butanol 41 56 i • ■ • • i ■ ■ ■ ■ i TTTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- m/z 42 05 68.21%

45 ........................................ 38 53 ■, ■ i' ■ ■ ■ i 1 ■ ■ ■ i ■ • ■ > i ■ ■ • ■ i • ■ ■ • i ■ > ■ ■ i > ■ • 11 > • ■ ■ i • • ■ ■ । ■ m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62310: Cyclobutane 41 4.90 5.00 5.10 5.20 5.30 5.40 5.50 56 m/z 43.05 60.04% 5000 27

TH38 49 53 11I > i । TIPWIPIIngr , i i |-m-rp-r +11.......... . m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26828.D NP112701.M Fri Dec 07 14:53:19 2001 Page 2

NYC-WTC_000032191

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