GCMS analysis results for sample AD27679, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033263–000033284

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC1901\27679.D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Pentanol, 4-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.12 2.27 ng/uL 504373 1,4-Dichlorobenzene-d4 11.85

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 33 2 1-Butanol / 74 C4H10O 000071-36-3 28 3 5-Methyl -5-hexen-3 -ol 114 C7H140 067760-89-8 23 4 Pentane, /2, 3-dimethyl - 100 C7H16 000565-59-3 17 Abundance / Scan 31 (5.124 min): 27679.D (-) m/z 41.05 100. 00% 41 56

5000

I'1 ‘1111 . 11 . iMpi.r,, 45 71 67 | 4.90 5.00 5.10 5.20 5.30 5.40 5.50 50 m/z-> 20 25 30 35 37. 51 Titr + TTTTTTTTT 40 45 50 55 60 65 70 75 80 85 rr >। I'' " I 100 TUI——turn 90 95 100 105 m/ z 56.10 75.19% Abundance #63578: 1-Pentanol, 4-methyl- 56 41 69 5000 TTTIT r '' ■ i TT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42,. 10 67.72%

m/z-> 20 25 30 i ■' * ■ । 4 L0— TT MM TTUIPunun 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 84

Abundance #62584: 1-Butanol 41 56 —OTTuUTTT 4 90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/ z 59.10 66.17%

45 i 37 h m/z~> m TIUUTT0B—I0—1011UC-IVVIIIUINIIUIEITITTTTTH1Im11 1 11 < ' 1 ’ I 11 1 ' 11 ‘ '11 1 1 1 1 I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #2990: 5-Methyl-5-hexen-3-ol pm-rp-r " I ' ' n I' ’ ' ' I ' ' ' ' I ' " rl' 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 43.05 61.56% 5000- 31 27 85 _N _ _ 11 r 42 51, 50 67 81 ''I'11' I' T’T TIIUNIITTHT 1111 * 1111111'1 ‘ I'' " 11 ’1 T1- • ’ I'' ’ • I “1 ’ I • •' ’ I ’' I m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27679.D NP112701.M Thu Dec.20 11:42:02 2001 Page 1

NYC-WTC_000033271

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GCMS analysis results for sample AD27639, Jan 2002 · Box DEP Box 21

NYC-WTC_000033221

Laboratory report documenting GCMS analysis of sample AD27639 for unknown compounds and surrogates on January 3, 2002.

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