GCMS calibration data, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC2 10128171.D Vial: 37 Acq On : 22 Dec 2001 1:59 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 5 2-Pentanol, 4-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.44 0.64 ng/uL 169133 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Pentanol,/ 4-methyl- 102 C6H140 000108-11-2 43 2 2-Pentanol/ 4-methyl- 102 C6H140 000108-11-2 43 3 2-Hexanoy 102 C6H140 000626-93-7 38 4 2,5 -Hexanediol 118 C6H14O2 _______ 002935-44-6 36 Abundance 7 Scan 610 (10.438 min): 28171.D (-) m/z 43.10 100.00% 4b ■ 1

5000-

85 1 - •X- / V

e I i । ■1 39 i 57 61 69 10.20 10.40 10.60 10.80 | — ■ । ■'' ■ । ■'' ■ ।' 4 TTTt m/ z 45.10 71.78% miz-> 20 25 30 35 40 45__ 50 55 60 65 70 75 80 85 90 95 Abundance #1773: 2-Pentanol, 4-methyl- ! 45 I

5000 -A- ■ ' f 1 TPA-Im 10.20 10.40 10,60 10.80

27 42 57 69 m/z 41.10 30.29% 1 I | 84 87 ' 11 11 THHm mBmpTri l ! | > > > I | I | m/z-> 20 25 30 35 40 45 50 55 60 65 7G 75 80 85 90 95 Abundance #63547: 2-Pentanol, 4-methyl- 45 — Am 10.20 10.40 10.60 10.80 5000- m/z 85.15 20.87% 27 69 - 57 • 84 87 TPTTITPTTT 11BI—gTgU m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 _________________ Abundance #63583:2-Hexanol ----- A IT 45 10.20 10.40 10.60 10.80 m/z .57.10 15.83% 5000

— 69 27 31 39 42 55 58 | 84 87 "Iptuur TTTT imrm T T111————mmmuaupTtmuTgm HAAA— miz--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 10.20 10.40 10.60 10.80

28171.D NP112701.M Fri Dec 28 09:07:43 2001 Page 5

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