GCMS analysis results for sample AD27276, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27276.D . Vial: 4 Acq On : 19 Dec 2001 8:56 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.49 2.02 ng/uL 487720 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol/ 4-methyl- 102 C6H140 000108-11-2 59 2 2,5-Hexanediol/ 118 C6H14O2 002935-44-6 59 3 2-Hexanol 102 C6H140 000626-93-7 53 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 53 Abundance / Scan 616 (10.488 min): 27276.D (-) m/z 43.10 100.00% 43 /

5000 85 T"T y 39 57 69 I ′ '' I

m/z-> Ib'' ■ I " 111 41 5344 61 -H tpr 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 T+ i' ’ " i ■ ‘ " (■' ■' i' ■ " i m/z 10.20 10.40 45.10 10.60 10.80 79.51% Abundance #1773: 2-Pentanol, 4-methyl- 45

5000 Tor 10.20 10.40 10.60 10.80 m/ z 29.89% - 27 T+++ 57 TTTHHT 11 >1 > ।! <'. । ।। 1*—*) TTT11 69 87 41:10 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #64444: 2,5-Hexanediol 45 ----- TTuni 10.20 10.40 10.60 10.80 56 5000 m/z 85.15 19.48% 41 ' 85 i 27 I II 67 1 r ■ ■ ■ r' ■' r i ■ ■' ■ r " ' i -p-i i i । . i TIT n i ji . ri 11 > r i TUBgOu—guonn m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexano! -A A-— 45 10.20 10.40 10.60 10.80 m/z 57.10 16.53% 5000-

— 69 ‘'I.. 47,31... . 55 '1111 Tm]]] I 87 TId —AA m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

27276.D NP112701.M Wed Dec 19 09:57:54 2001 Page 5

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