GCMS method parameters and calibration table, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\LB.D Vial: 2 Acq On 18 Dec 2001 4:49 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.51 1.52 ng/uL 414732 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentano1, 4-methyl- 102 C6H140 000108-11-2 59 2 2-Hexanol 102 C6H140 000626-93-7 53 3 2-Hexanol 102 C6H140 000626-93-7 53 4 2-Pentanol, 4-methyl-______________ 102 C6H140 000108-11-2 53 Abundance = Scan 618 (10.513 min): LB.D (-) m/ z 43.10 100.00% 43

5000-

57 85 ' ' p ■ ''i1 TT

m/z-> 20 m 39 Tpr 5344 61.. .I.. . 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 100 TTTH +]TT 10.20 10.40 10.60 10.80 m/z 45.10 89.56% Abundance #1773: 2-Pentanol, 4-methyl- 45

5000 —frr L....... 10.20 10.40 10.60 10.80 69 m/ z 41.10 32.78% 27 57 ----- - ‘IT TIHH I *IBaUuur 87 TTITTT T TTTTT ,.., TIT., TUT] m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1792: 2-Hexanol 45

10.20 10.40 10.60 10.80 5000- m/z 85.15 19.82%

55 69 TTT 27,31 39 . 1 87 TTT TT i " " i' "' i " " i TTTTTTTTTTTTTTprm] m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexanol 45 ' ' I ' 1 10.20 10.40 — -A 10.60 10.80 m/z .57.10 16.82% 5000 -

27 31 TTTTT 39 , — > > i ■ ■ ■ ■55 69 1111. ।.... ।. 111,.. ■ ।.... ।...' । ■87 i.. ।.... ।.... ।.... ।.। • ■ i • ■ • ■ I • . A i ■1 ■ ' i 1 ■ 1 ■ । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

LB.D NP112701.M Thu Dec 20 11:38:01 2001 Page 4

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