GCMS analysis report, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28308.D Vial: 40 Acq On : 22 Dec 2001 4:43 pm Operator: GALOS Sample : gems unknown 11/26 Inst ■ : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C : \DATABASE\NBS75K . L ********************************************************************* Peak Number 2 2-Pentanol, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.74 0.46 ng/uL 124418 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentan , 4-methyl- 102 C6H140 000108-11-2 83 2 2 -Hexand 102 C6H140 000626-93-7 83 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Hexanol 102 C6H140 000626-93-7 74 ‘Abundance Scan 207 (6.741 min): 28308.D (-) m/ z 45.10 100.00% 45

5000- .............. - 11 41 69 6.40 6.60 6.80 7.00 57 | 84 87 —..........- TIHTT TIPPTTIWWTIPWNTTTTTTTTTTTTT m/Z 69.10 14.55% miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1773: 2-Pentanol, 4-methyl- 45

5000 —4 6.40 6.60 6.80 7.00 69। m/ z 41.10 14.07% 27 42 57 84 87 1 i■■■■i■' i■ ■' ■ i■'' ■ i' "' i1 11111 TTtrrTIT T P TTTT ■ । ■1 ■ • । >11»i > • । • • * ■ । ■ m/Z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexano! 45 W , I Y 6.40 6.60 6.80 7.00 5000 m/ z 43.10 12.00%

69 19 27 31 42 i 56 | 84 87

AAR TT TTTTTT 111111111111111111।।।।।।। ।।।r m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundancei #63547: 2-Pentanol, 4-methyl- 'r — r 45 6.40 6.60 6.80 7.00 m/ z 44.10 10.79% 5000 -

miz-> .... 38.14— i" i ■" ■ i •1" i ■ 10 15 20 25 30 35 40 27 nmPmp 57 45 50 55 60 65 69 | 84 87 •। ><>■।■ ■ ■■j■•■ •।•I >■ । 70 75 80 85 90 •I•■ 95 Al A 6.40 6.60 6.80

28308.D NP112701.M Fri Dec 28 09:09:32 2001 Page 2

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