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GCMS analysis results for sample AD27627, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27627 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033143–000033158

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033154
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NYC 9/11 Public Portal Document

Library Search Compound Report

■Data File : C:\HPCHEM\l\DATA\DEC1901\27627.D Vial: 17 Acq On : 20 Dec 2001 12:30 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.82 1.28 ng/uL 405955 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Pentapfol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Hexanol 102 C6H140 _________ 000626-93-7 74 'Abundance Scan 216 (6.822 min): 27627.D (-) m/z 45.10 100.00% 45

5000 - ..........-......................... 41 69 6.40 6.60 6.80 7.00 7.20

m/z-> ।■■■■।"■■ । ■"11'1111'11111 +4 WImuumm—gTTT ' l ■ ■ ■ ■ 1...84 .50535659........... 1 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 11 ■87 l • • I ■ • ■' I • m/z 41.05 14.17% Abundance #63547: 2-Pentanol, 4-methyl- 45

T’IE-TT/—ET—TETETTIIUF 5000 6.4C 6.60 6.80 7.00 7.20 27 69 m/ z 69.10 14.09% 38 42 ■ i111 57 | 84 87 , (.... ।~। T TIWTTUT TTTT 11 . L . i.... j. । m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45 4 6.40 6.60 6.80 7.00 7.20 5000 m/z 43.05 12.90%

69 19 11 T‘ ITTTTTr 27 ,31 42, 56 84 87

A ' i ■ ■'11 ■ ■ " r " 11 ‘1 ■' I'111111 " I " 111'1 " 11 " ' r ''' i ■ TIUTTg mlz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 8.34% 5000 -

miz-> 10 15 20 19 25 27 31 — 30 42

35 40 45 1 57 84 87 nmHH 11WTITTTTHTTTI 50 55 60 65 69

70 75 80 85 90 95 .AAAAs 6.40 6.60 6.80 7.00 7.20

27627.D NP112701.M Fri Dec 21 09:18:15 2001 Page 4

NYC-WTC_000033154

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NYC-WTC_000033154Source: NYC Law Department, mirrored locally

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