GCMS analysis results for sample AD27569, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC13 01\27569.D Vial: 10 Acq On 13 Dec 2001 6:34 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area’ Relative to ISTD R.T.

10.50 1.14 ng/uL 342055 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, A-methyl- 102 C6H140 000108-11-2 64 2 2-Hexanol / 102 C6H140 000626-93-7 59 3 2-Pentanol, 3-chloro-4-methyl - , (R@ 136 C6H13C1Oi 074685-47-5 50 4 2-Hexanal 102 C6H140 000626-93-7 50 Abundance Scan 617 (10.499 min): 27569.D (-) m/z 45.1.0 100.00% 45

5000 - 41 69 85 57 61 10.20 10.40 10.60 10.80 — — T TT+53 100 TTTTTTTTTrm) m/ z 43 • 05 92.87% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1773: 2-Pentanol, 4-methyl- 4(5

5000 - 1′1 10.20 10.40 10.60 10.80 69 m/ z 41.10 31.32% 27

m/z-> 20 m 25 30 35 T 40 45 57 ....... 4 50 55 60 65 70 75 80 i • • • • i"1 • I 1 87 85 90 I" " I 95 100 105 Abundance #63583: 2-Hexano! 45 X 1’1,/ TII Pr — fr i 10.20 10.40 10.60 10.80 5000 - m/ Z 85.0.5 18.07%

69 27 31 -rm-p-rr-ry 39 . , "i" "I 55 I i ■ ■ " i'' " r " • i 87 TVNuppuumn m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #6421: 2-Pentanol, 3-chloro-4-methyl-, (R@,R@)-(.+/-.)- 45 ' 'I1' _____ \ —A ’-1 , TT-r r-j-r 10.20 10.40 10.60 10.80 m/ z 57 • 10 16.60% 5000-

27 58

miz-> TPTTTTPTTTTTTTTT —H 69 76 T-p-rrIUOOT——TTTup-n-rp-rrr] 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85 100 ■ ■ i ' 44 AA 10.20 10.40 10.60 10.80

27569.D NP112701.M Fri Dec 14 12:58:03 2001 Page 4

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