GCMS analysis results for sample AD27569, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27569.D Vial: 10 Acq On 13 Dec 2001 6:34 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.29 1.02 ng/uL 304568 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexan 102 C6H140 000623-37-0 50 2 Silane/ trimethyl- 74 C3H10Si 000993-07-7 47 3 3-Hex. nol 102 C6H140 000623-37-0 42 4 3-He: nol 102 C6H140 _______ 000623-37-0 42 Abundance Scan 594 (10.289 min): 27569.D (-) m/z 43.10 100.00% 43 59 55 5000 73 39 85 T’T

m/z-> rJr 4 I 4 Hl+ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 TT 100 p............ 10.00 10.20 m/ z 59.10 10.40 10.60 72.21% Abundance ..... #63528: 3-Hexanol 55 59 . 73 5000 -- 1 ---A- — r 31 10.00 10.20 10.40 10.60 27 m/z 55.1.0 56.38% 45 1 r'b • i +4 TT TH 1’11117 ''I i" • ■ i" ।■ i T‘ + 84 m/z-> __ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #331: Silane, trimethyl- 5.9 I -A 10.00 10.20 10.40 10.60 73 5000- m/z 41.10 41.00%

45 33 I 55 j l T’TTTTTT’T r ■" i" " i ■ i ■ ■' I' " ' I' •'' I'1 ‘11111' I'1 •' 11'1' I i" " i T‘ m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol ■ ■ i ■ TIT

55 59 m/z 10.00 10.20 10.40 10.60 57.10 36.71% 31 5000 73 27

44 mmHH +44 . ............ ___________________ " ! " " I' TT TTTTmIuuuIu—102 BTIO"TR‘ MA 4 4 A m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 10.00 10.20 10.40 10.60

27569.D NP112701.M Fri Dec 14 12:58:01 2001 Page 3

NYC-WTC_000033531