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GCMS analysis results for sample AD27550, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27550 conducted on December 18, 2001.

NYC-WTC_000033505–000033520

Folder label: “GCMS X 11/15/01 A 12/13/01

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Scanned page image, NYC-WTC_000033518
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1301\27550.D Vial: 9 Acq On 13 Dec 2001 5:39 pm Operator: GALOS Sample : gems unknown 11/15 •Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.50 1.29 ng/uL 527510 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 59 2 2,5-Hexanediol 118 C6H1402 002935-44-6 59 3 2-Hexanol 102 C6H140 000626-93-7 53 4 2-Pentanol, 3-chloro-4-methyl-, (R@ 136 C6H13C1O 074685-47-5 42 Abundance Scan 617 (10 498 min): 27550. (-) m/z 43.10 100.00% 4b

m/z-> 5000

r "' I 39 41 —pr 5344 H 57

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 85 100 TPWTTTHT TTTmTTu .............. _ A T-T-f-1 it TICIIT1T8 10.20 10.40 10.60 10.80 m/ z 45.10 £ 92.50% Abundance #1773: 2-Pentanol. 4-methyl- 45

5000 - / 1 ■ 'I 10.20 10.40 10.60 10.80 69 m/z 41.10 32.42% 27 m/z—> — —+ TIPPT THT •... 57 1.......... ................ 87 r * • ‘ r "11 •" • i • • • ‘ i •1 “ P TTTTTT 1111111j 11111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64444: 2,5-Hexanediol 45 / ■ • i ' ' Aen 10.20 10.40 10.60 10.80 56 5000- m/ z 85.05 19.47% 41 85 27 67 iii________________________________________________________________ TTDT . T‘‘‘‘01‘1T‘"T‘TT‘‘1‘11000100100TTTTOIt‘TM mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583:2-Hexanol ■ ■ । ■ ■ 45 10.20 10.40 10.60 10.80 m/ z 57.10 17.13% 5000

69 27 31 39 _ , — — 4XA 55 87 " I"" 1111111111111 >111111 TTHmm T I I . . 1 . . . . ) . 1 ) . I . . ( 4I I I |<■>, | I I I I | I ! I<| m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

27550.D NP112701.M Fri Dec 14 12:57:30 2001 Page 6

NYC-WTC_000033518

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NYC-WTC_000033518Source: NYC Law Department, mirrored locally

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