GCMS analysis results for sample AD27276, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27276.D Vial: 4 Acq On 19 Dec 2001 8:56 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.49 2.02 ng/uL 487720 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 59 2 2,5-Hexanediol 118 C6H14O2 002935-44-6 59 3 2-Hexanol 102 C6H140 000626-93-7 53 4 2-Pentanol, 4-methyl-__________ _ 102 C6H140 _____ 000108-11-2 53 'Abundance Scan 616 (10.488 min): 27276.D (-) m/z 43.10 100.00% 43

5000

57 85 TITT 69

m/z-> l39 TT‘ 534161 —....r1+ 20' 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 m/z 10.20 10.40 10.60 10.80 45.10 79.51% Abundance #1773: 2-Pentanol, 4-methyl- 45

5000 R ।11' 1^' ' ' P' ’ ' 10.20 10.40 10.60 10.80 69 m/ z 41.10 29.89% 27 5787 , — . , - — T 1 "ITTTHHH TT ।।.... । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64444: 2,5-Hexanediol 45 । । । । ------P । i-1 — 10.20 10.40 10.60 10.80 56 19.48% 5000 m/z 85.15 41 85 27 67 TCTUIIWWTTTT)WUTTTTTNUTTTTT i ■I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 45 #63583: 2-Hexanol 10.20 10.40 10.60 A 10.80 m/z 57.10 16.53%

5000

— 69 27 31.. 39 TIIUTTTTTTTWTTTTTT 55 | 87 i11 " 1 i | Hl111 >!! 11! 111 n TIT ... ।. i > 11.1., ।...., > TTTpr 1111 111 - i 2A 1 1 I IBA m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

27276.D NP112701.M Thu Dec 20 11:38:38 2001 Page 5

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