GCMS analysis results for sample AD27679, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27679.D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 2-Hexanol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.88 ng/uL 196184 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Hexanol 102 C6H140 000626-93-7 72 2 2-Pentanol , 4-methyl- 102 C6H140 000108-11-2 64 3 2-Pentanol , 4-methyl- 102 C6H140 000108-11-2 56 4 2-Pentanol, 4-methyl- 102 C6H140 _________ 000108-11-2 50 ■Abundance Scan 215 (6.811 min): 27679.D (-) m/z 45.10 100.00% 45

5000- 41 56 69 72 84 87 ..... Al 6.40 6.60 6.80 7.00 7.20 -IPTTTTTTTT + H I ‘1 ■ * r ' ■ TITT TT TIPTTT m/z 41.10 22.51% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583: 2-Hexanol 45

5000- 6.40 6.60 6.80 7.00 7.20

69 m/z 43.05 20 10%

m/z-> .... 431...^-1- 20 25 30 35 40 55 58 TTPTTNT) 45 50 55 60 | TI9BTmReng 65 70 —84 87 pun]r 75 80 85 90 95 Abundance #63547; 2-Pentanol. 4-methyl- 45 A_/ — 6.40 6.60 6.80 7.00 7.20 5000- m/z 44.05 17 97%

27 69

AL 38 42 57 84 87 ■ ■ । ■ ■ ■ ■ ।' ' i1 ■ ■ ■ i1 ■'' I'1 •11' TTT i , > | < i-n j i i > ; | > > TTPPTTT I I I | < i l 1I—PBI—gr m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545: 2-Pentanol, 4-methyl- MA —Y 45 6.40 6.60 i6.80 7.00 7.20 m/ z 69. 13.88% 5000 10 69

m/z-> — ।।.1 27

20 25 30 39 42 . I j. 11 + 35 4G 45 TTT TH 57 50 55 60 65 4 70 84 87 ■ l1 ■ i''11TTIT ■ ■ i ■ ■ 75 80 85 90 95 ........... A4 6.40 6.60 —

6.80 7.00 7.20

27679.D NP112701.M Thu Dec 20 11:42:16 2001 Page 8

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