GCMS analysis results for sample AD27627, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC1901\27627.D Vial: 17 Acq On 20 Dec 2001. 12:30 pm Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.87 ng/uL 277286 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 _ Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-H anol 102 C6H140 _______ 000623-37-0 83 Abundance a Scan 204 (6.712 min): 27627.D (-) m/z 59.10 100.00% 59 55

5000 73 43 --------------------- 39 6.40 6.60 6.80 7.00 111 - 84 -rp-rrr 44 PPp 1T T’T I " ‘ ’I TIT"TTVTTT‘‘TT m/ z 55.10 78.44% m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol 59 55 31 5000 - 27 43 73 r n 111 '~i 6.40 6.60 6.80 7.00 m/z 73.0.5 38.38% 102 m/z-> TTT r ''' i TTTTTT TT 11

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 4 Abundance #63527: 3-Hexanol 59 55 I I ' ' ' ' I ' ' ' ' I 6.40 6.60 6.80 7.00 73 m/ z 10 31.57% 5000 31 43- 27 45 84 <II T’TTTT’TTTT TTTT i1 ■ " i ■ " 11' ‘" i " " r "' i" " i " " i" " i'' 111 > > > I >. ITTTTTT T’ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanol l ■ j • ■ 1 ■ l

55 59 6.40 m/ z 6.60 41.10 6.80 7.00 23.08% 5000-

m/z-> " i " " r' " r ' " I 39 ... H 43 . 11 , 69 , 73

' | 1 ' 1 1 | I । 1 । | Illi | I < I I | I M I | I I I I | I lll| I I ( I | I l t TT’’"’ITTTT [ I « I ( | I

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Ju 6.40 6.60 6.80 7.00

27627.D NP112701.M Fri Dec 21 09:18:13 2001 Page 3

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