GCMS method parameters and calibration table, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\LB.D Vial: 2 Acq On 18 Dec 2001 4:49 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.30 1.18 ng/uL 324101 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# ' Qual

1 3-Hexanol 102 C6H140 000623-37-0 37 2 3-Hexanol 102 C6H140 000623-37-0 37 3 3- anol .102 C6H14O 000623-37-0 37 4 3-Hexanol 102 C6H140 000623-37-0 25 (Abundance 43 Scan 595 (10.302 min): LB.D (-) m/z 43.10 100-00*

55 59 — 5000-

39 73 85 ' 1 I L ■ i ' ' P 10.00 10.20 10.40 10.60

m/z-> i < ■ ■ ■ i ■ ■ ■ > । 1 X X™ Hl 11 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/z 59.16 58.43% 'Abundance #63527: 3-Hexanol l................................. .. 59 55

5000- 73 31 10.00 10.20 10.40 10.60 m/ Z 55.10 ■ 50.46% 27

m/z-> Tp ...... 45..... 4 20 25 30 35 40 45 50 55 60 65 70 75 80 TT 84 i' " ' i i ■ ■ ‘■ i ■ ■ ■ ■ i ■■ ■ •। 85 90 95 100 105 110 TT

Abundance #1762: 3-Hexanol ' 59

31 55 ' 10.00 10.20 10.40 10.60 LX If 5000- 27 43 73 m/z 41.10 36.96%

! .Il . 102 ' ’ i " ■ -1 ■" ’ i ■ *' ■ i " " i TTTTTTTTTTTTTTT i ■ ■ ■ ■ i i ■''' r “ ' i " '' r ' " i i •1" i TT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 'Abundance #63529:3-Hexanol ■ ' i '

55 59 10.00 m/z 10.20 10.40 10.60 57.10 36.96% 31 5000- 73 27

" i " ‘' r TI 44 -H 44 mp 1 r 11' i1" ■ r '' ‘ i ‘' i 102 i " " i " " 11 1 1 ' i ' ' ' 1 i ' 1 ' 1 i ' AR4 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 10.00 10.20 10.40 10.60

LB.D NP112701.M Thu Dec 20 11:37:59 2001 Page 3

NYC-WTC_000033039