GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Hexanol Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.63 0.50 ng/uL 107868 1,4-Dichlorobenzene-d4 11.80

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H14O 000623-37-0 83 2 3-Hexanol 102 C6H14O 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3 -Hexanol 102 C6H140 000623-37-0 64 Abundance Scan 195 (6.634 min): LB.D (-) m/ z 59.10 100.00% 55

5000 73 43 . ....... Ar • miz-? i TT r 20 25 30 35 39 4 40 LL 45 ' • 11 ' 50 +55 ■ ।. .. . । . . . . । . I 60 65 70 ' l' • ■ ■ l ■ • ■ • l • ■ • ■ I ■ • 75 80 85 90 6.20 m/z 6.40 6.60 55.10 6.80 7.00 ..... 77.24% Abundance #63527: 3-Hexanol 55 59 5000 31 73 ■I —— 4A AA 6.20 6.40 6.60 6.80 7.00 m/z 73 • 0.5 37.90% 27 | 45 . 84 1111 ■ ■ ■ । ■' ■ ■ ।1 ' ' I " ' ' I ' ' ' ' I ' " ' I '1 1 1 1 | > 1 1 > | i • 1 । | m-r p > i i । > i > i । i i i . ) < > < > । i i m/z—> „ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance 59 —................ — 55 6.20 _ 6.40 6.60 _ 6.80 7.00 _ 73 5000 m/z 43.10 26.33% 31

27 84 45 m/z- > Abundance T‘T‘‘*110uuunpTu TTT‘II———10TTOITVOVIIIITTTTT 20 25 30 35 40 45 50 55 #63531: 3-Hexanol 55 59 60 65 70 75 80 85 90 —.,A— —— 6.20 m/z 6.40 41.10 6.60 6.80 7.00 22.93%

m/z-> 5000

39 । 43 . , .............. 39, —IPWTTTTTTTTIMTN TTI’turu " i" 11 ■ ■ ■ ■ i'' ■ ■ P ■' ■ i ■ ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 73

NA 6.20 MW. 6.40 6.60 6.80 7.00

LB.D NP112701.M Fri Dec 28 11:46:49 2001 Page 4

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