GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 2-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.74 0.75 ng/uL 163024 1,4-Dichlorobenzene-d4 11.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Hexanol, (R)- 102 C6H140 026549-24-6 74 Abundance Scan 207 (6.744 min): LB.D () ....... !.m/z .45.10. loo 00% 45 i T 1

5000

1‘13———OOTT. 41 69 57 6.40 6.60 6.80 7.00 1 84 87 1...................... H HHmp TTWTTTTTTIWWTTUTTTNTIWTTTT’T m/z 41.10 14.55% m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance

5000

19 27.31 42 56 #63584:2-Hexanol 45

84 8/ ‘T‘ ‘OUUmuumninuunnnnnnnuT T TTT........ i' " ■ i■'1' r ■ ■11''■■i " ■' i ■1 69 N

m/ z JW._ 6.40 6.60 69.1.0 6.80 7.00 14.21%!

m/z->___ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 2-Hexanol 45 TT 6.40 6.60 6.80 7.00 5000 m/ z 43.05 ” 12.93%

27 31 3942 55 58 69 84 87 l.... ।..., ।,... ।,.., ।,. >. ।.. >. ।. t. ।....,..., ।. j . ।, • i ■ ■ ■ 11" " i ‘ " i1 " i " i " ' ■ i ■ - m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547: 2-Pentanol, 4-methyl- 1 । < ... । i i । 1 । i । । 45 6.40 6.60 6.80 7.00 j m/ z 44.10 ' 9.76% 5000

27 69 . ................................................ - .. ........ . | 84 87 ■ r " ■ r " ■ r ’ " i ■' ■' i'1" i' " ' i' miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

LB.D NP112701.M Fri Dec 28 11:46:51 2001 Page 5

NYC-WTC_000034572