GCMS analysis results for sample AD27954, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27954.D Vial: 10 Acq On : 21 Dec 2001 12:22 am Operator: GALOS Sample : gems unknown 11/20 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.80 ng/uL 259352 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Hexanol 102 C6H140 000626-93-7 83 4 2-Pentanol, 4-methyl- 102 C6H140 ____ 000108-11-2 83 Abundance Scan 215 (6.811 min): 27954.D (-) m/z 45.10 100.00% 45

5000

41 69 i • ■ • 1 i ■ 84 87 6.40 6.60 6.80 7.00 7.20 miz-> mmmm.......... +4 .....5558...... 1..... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z I I| I I J| III I| I I M | I I 69.1,0 14.14% Abundancei #63582: 2-Hexanoi 45 i

5000 | 6.40 6.60 6.80 7.00 7.20 i 27 69 m/z 41.10 13.89% 31 4; 84 87 19 TTh T TH ■ > । •1 > | 57

Md. r ■ ■ ■ i ’''' i' • 11. ।.... ।' 11' ■ ■ > ।।।" 111 r 111111.111 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583: 2-Hexanoi 45 PAP 6.40 6.60 6.80 7.00 7.20

4 5000 m/z 43.05 11.35%

27 31 3942 5558 69 84 87 I । ।।I "i 11111 >> 111 ■ ■■ 1111111 •i" । ■111TTT > 1111111111111 m/z- . 10 15 20. 25 30 35 40 45 50 55 60. 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol . . p I T I । . 1- l 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 9.80% 5000

69

miz-> 111■■ ■ । 10 15 20 19। ■1 ■■।■27,31 I■111 ■ ■ 25 30 —4 56 ............. 111"! 35 40 45 50 55 60 ‘I‘ 65 80 84 87 11' ■ ■ ■ i' ■ ■ ■ i ■ " 11 ■'111111111 70 75 85 90 95 -AAA. ,4 AA, AA.4 6.40 6.60 6.80 7.00 7.20

27954.D NP112701.M Fri Dec 21 09:59:21 2001 Page 4

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