GCMS TCLP calibration table, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\LBB.D Vial: 3 Acq On : 20 Dec 2001 5:58 pm Operator: GALOS Sample : gems unknown 11/20 Inst - : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Hexanol, (R)- Concentration Rank 3

R.T EstConc Area Relative to ISTD R.T.

6.81 0.73 ng/uL 286493 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 'Tentative ID MW MolForm CAS# Qual

l 2-Hexanol, (R) - 102 C6H140 026549-24-6 83 2 2-Hexanod 102 C6H140 000626-93-7 64 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 Abundance Scan 215 (6.814 min): LBB.D (-) m/z 45.10 100.00% 45

5000 i11 — — 41 69 6.40 6.60 6.80 7.00 7.20 84 87 4 ................. 1...... miz->10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z .. ।... 11.1.. ।.... ।.. 41.10 13.38% Abundance #1794: 2-Hexanol, (R)- 45

5000 6.40 6.60 6.80 7.00 7.20 m/ z 69.10 13.31% 69 19 129 3942, 55 | 84 87 TTTTTTOWTTTTTTITUTTSTUIITTOTITT "IUUuIuuuuwuuutOuuutmornprrrmn miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792: 2Hexanol 45 ______ A X_________ I ' ' ' ‘ I • ‘ ' I ■ ■ ' ' I ' ' I ' ' 6.40 6.60 6.80 7.00 7.20 5000 m/z ,43.10 12.36%

27 31 3942 55 58 69 84 87 ————— .(TT-rr-p-rT-rp, TILWn—BpTtgr i . . p i , q . I m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1773: 2-Pentanol, 4-methyl- “ ~ ........ TT ----- • 45 6.40 6.60 6.80 7.00 7.20 m/ z 44.05 8.35% 5000

27 69 42 57 | 84 87 ................ -n-f T -m-p TII WTIppudtumhur j ,i i 11’1 tTTTTT —AMAr miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

LBB.D NP112701.M Fri Dec 21 10:01:09 2001 Page 4

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