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← Document results/DEP Box 22/GCMS X 11/20/01 A 12/20/01
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GCMS TCLP calibration table, Dec 2001

Machine-extracted title · confidence 95%

Calibration table for TCLP analysis listing retention times and response factors for standard compounds on December 20-21, 2001.

NYC-WTC_000034006–000034017

Folder label: “GCMS X 11/20/01 A 12/20/01”

←Page 9 of 12→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\LBB.D Vial: 3 Acq On : 20 Dec 2001 5:58 pm Operator: GALOS Sample : gems unknown 11/20 Inst - : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.49 ng/uL 194506 1,4-Dichlorobenzene-d4 11.86

Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 3-Hexa: 61 102 C6H140 000623-37-0 83 2 3-Hexal ol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance/ Scan 203 (6.704 mln): LBB.D (-) m/z 59.1.0 “100.00% 55 59

5000 73 43 39 6.40 4 6.80 7.00 6.60 I 1 ’ 1 'I ' 1 ‘ ' I

m/z-> i " " i" ■ ■ i mH Tp-r + tTTTTTT I I I | I l 11 . H . p h . I । 11 I l p l . . । . . . . । . . . . । . . . . । . 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/ z 55.10 83.27% Abundance #63528: 3-Hexanol 55 59

73 5000 ■ ■ i ■ ■ ■ • i 31 6.40 6.60 6.80 7.00 m/z 73.05 43.40% 27

miz—> ... H l""l + 45 . ..... TT r "' i + ) > • I * |l III | • I I I | M M | f

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 84

Abundance #63527: 3-Hexanol — 59 55 T-r-j-r-r-r-r-|-rT ■ \ ___ ■ i ■ ■ ■ ‘ I 1 1 1 1 I 6.40 6.60 6.80 7.00 5000 73 m/z 43.10 30.62% 31 1 |i 27 45 84 .. । . . , , । , , , , । , , ,, t, , , , । , ,, , । , , , ., , ,, , । . , , , | . ., . । , , , ,,. , ‘ITIITTTTTTTTT ’ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol ■ " ‘ I • • I ■ I ■ » n-J i-i-i-r | . i . . | i 59 6.40 6.60 6.80 7.00 ? 55 m/z 41.10 23.22% 31 5000 27 43 73 __

________________ 102 i" " i pp TT‘‘"O—EI0"11—0‘"IUITC—T"OuITr miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00___

LBB.D NP112701.M Fri Dec 21 10:01:07 2001 Page 3

NYC-WTC_000034014

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NYC-WTC_000034014Source: NYC Law Department, mirrored locally

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