GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.50 1.12 ng/uL 242562 1,4-Dichlorobenzene-d4 11.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 90 Abundance 4|3 Scan 180 (6.496 min): LB.D (-) i m/z 43.10 100.00%

58 5000

100 A 6.20 I | I TH I pl TT I | : 6.40__ (6.60 6.80

m/z-> ......... l +.....TH 53 | — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71 85 PT ...... | n i 111 i > 11 m/z 58.10) 55.06% Abundance #63386:2-Hexanone 43

5000 58 1 ■ i 1 1 ■ ■ 11 __ 6.20 6.40 6.60 6.80____ ; 29 m/z 41.10 14.98% 100 m 71 85 P..... I

A TTtti l ■ ■ ■ • I" TT I ■ " ■I m/z->____ 20 25 30 35 40 45 50 55 60 65 .70 75 80 85 90 95 100 105 Abundance ■ 54 2-=cxane s 43 I I • ' ' ’ I ’ ' ' ' I * ‘ 1 • 11 6.20 6.40_ 6.60 6.80 । 5000 58 m/z 57.. 10 14.49% 29 39 71 85 100 I"" I 1 "‘I"'U""I I .... | >1 U|I. .I| miz-?... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 43 T

#63385: 2-Hexanone -M ____6.20 m/z 100.15 6.40 6.60 r TI Prr 11 6.80 8.84% !

5000 58 29

miz- .. I.!,... m 39 p +T 71 85 11 •" i1"' i " " r " ■ r " ■ r " ' i" " i'''' i 20 25 30 35 40 45 50 55 60 65 . 70 75 80 85 90 95 100 105 100 .... —A 6,20 6.40 6,60 6,80 __ J 1 1 1 ' 1 1 1'

LB.D NP112701.M Fri Dec 28 11:46:47 2001 Page 3

NYC-WTC_000034570