GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 3-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.40 0.67 ng/uL 144116 1,4-Dichlorobenzene-d4 11.80

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H12O 000589-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 83 4 3-Hexanone 100 C6H12O 000589-38-8 56 Abundance Scan 169 (6.395 min): LB.D (-) m/z 43.10 100.00% 43 57

71 5000 100 • I 1 ' । (Tr r _6.00 6.20 6.40 6.60 6.80 : m/z-? mm 4 t..........I1 53. 1 TT TTITTTTTTTT . ।.... । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 l" " I m/z 57.10 91.85% /Abundance #63358: 3-Hexanone 42 57

71 5000 TTA ITP 6.00 6.20 6.40 6.60 6.80 100 m/ z 71.05 59.24%' . 111••• I • •. 11.... I 85 i TT I" n I 1" " r • •' i i' " ' i" " I" " i" ■' i'' ■' i1 ”' i''" i miz-2 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 •Abundance

5000 29 43 . 57

71 6.00 m/z 6.20 41.10 I. 6.40 6.60 6.80 33.23% 100

W. 85 ‘I 111 I.«111.... I i" " i"k ‘ i "' * i TTTTCTTTTTTTT, miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357: 3-Hexanone 43 57 6.00 6.20__ 6.40 6.60__ 6.80 29 i m/z 10 0.05 30.27% 5000 71

m/z-> 85 mpTTTTTTmmTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 . A. 6.00 6.20 6.40 6.60 6.80

LB.D NP112701.M Fri Dec 28 11:46:45 2001 Page 2

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