GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Propene, 2-fluoro­ Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.14 0.45 ng/uL 98014 1,4-Dichlorobenzene-d4 11.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propene, 2- uoro- 60 C3H5F 001184-60-7 9 2 1-Butanol 74 C4H10O 000071-36-3 9 3 1-Propene 2-methyl- 56 C4H8 000115-11-7 7 4 Guanidi 59 CH5N3 000113-00-8 5 Abundance Scan 32 (5.139 min): LB.D (-) m/z 100.00% -143 56 59

5000 39 71 4 4a, AAA 45 5.00 5.20 5.40 5.60

m/z->.............20 25 30 35 40 J45...... 50 +55 60 i ' 1 1 1 I 1 ■ ' ■ i 65 70 ' ■ 1 i 1 75 80 m/z 43-16 91.66% Abundance #62355: 1-Propene, 2-fluoro- 59

39 A AA 5000

i ___ 5.00____ 5.20___ 5.40 5.60 27 3133 45 57 i m/ z 56.10 89.80% ■ ■ ■ i ' ■ ■ ■ i 1 ‘ ' ■ i ■ ■ ' ' i ' — 61 miz->..... ...... 20 25......30 35 40 45 50 55 60 65 70 75 80 Abundance 584; 1-Buture 41 56 43 I 1/ —5.40 T----- 5.60 — 5.00 5.20 5000 m/z 59.10 78.06%

39 45 37 53 ' i ' ■ ■ ■ i ■ ■ ■ ' i ' ' ' ' i ■ ■ ■ ■ i ■ ' ' ■ i ■ ■ ■ ■ i ■ 1 1 1 1 1 ' 1 ' I 1 1 1 1 i ' ■ i ' ■ ■ ■ i ■ ■ ' ■ i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62304: 1-Propene, 2-mefhyi- A A 41 ___ 5.00__ 5.20 5.40 5.60 m/z 4 2.10 74.99% 56 5000 39

2729 ■ 1' ' ■ 11 ■ • ■ ■ 1 ■ ■ • 1 1 ' ■ ' TT1 i + *P 53 ।111111111'111 i 1 ■ ■ 1 i A 1 ' 1 A— m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80_ 5,00___ 5.20 5.40 5.60

LB.D NP112701.M Fri Dec 28 11:46:43 2001 Page 1

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