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GCMS analysis results for sample AD29787, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29787 conducted on January 7, 2002.

NYC-WTC_000036995–000037006

Folder label: “GCMS X 12/10/01 A 12/15/01

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Scanned page image, NYC-WTC_000037005
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29787.D Vial: 12 Acq On 15 Dec 2001 1:16 pm Operator: 209 GALOS Sample : gems, scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ************************************* ** ** ************************** * * Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.35 ug/1 323641 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-m hoxy-l-methylet 148 C7H1603 020324-32-7 83 2 1-Propanol, 2- (2-h droxypropoxy) - 134 C6H14O3 000106-62-7 53 3 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 50 4 2-Propanol, 1,1 /-oxybi s- 134 C6H1403' 000110-98-5 39 'Abundance ■ Scan 695 (11.422 min): 29787.D (-) m/z 59.05 100.00% i 59

5000 45

73 103 M 11.00 11.20 11.40 11.60 11.80

mlz-> 20 ‘I" I I s p- ’30 +31451.4 40 50 H TIT (60 70 80 85................ ........................................... 90 100 110 120 130 | 140 m/z 44.95 49.63% 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 35.48% ------- .............................. i , ....................130............ — m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 i ' ■ > l ■ ■ • ■ l ■ ■ • ■ I ■ r 11.00 11.20 11.40 11.60 11.80 5000 m/ z 73.00 27.47% 31 45 103

■ ... 75.... 89 I ' I ’ ' ' ' I ' ' ' ' I ' m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 59 11.00 1120 1140 11.60 11.80 m/ z 41.05 26.20% 5000 - 31 45 103

m/z-> . ■ i ■ • ■ > । 20 30 .1 • i ' ' ■ . । . 40 50 t 60 70 80 90 100 110 120 ..... 134 130 140 TrrtT 11.00 11.20 11.40 UN 11.60 11.80

29787.D GCMS1126.M Fri Dec 28 13:22:55 2001 Page 4

NYC-WTC_000037005

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NYC-WTC_000037005Source: NYC Law Department, mirrored locally

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