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GCMS analysis results for sample AD29930, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29930 conducted on January 7, 2002.

NYC-WTC_000037029–000037039

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29930.D Vial: 8 Acq On 15 Dec 2001 9:22 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************** * * * **** *** * * ******** ** * * * * * Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 1.18 ug/1 309761 1,4-Dichlorobenzene-d4 . 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2ymethoxy-l-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3’oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1 -/2-methoxypropoxy)- 148 C7H1603 013429-07-7 53 4 1-Propanol, 2 / (2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 'Abundance Scan 686 (11.339 min): 29930.D (-) m/z 59.05 100.00% 59

5000

m/z-> -AL51 20 30 40 45

50 ■ 444 - — 60 70 ■ i1 80 90 73 103

89............ ।...................... 100 110 120 130 130 140 11.00 m/z 11,20 45.05 N 11.40 11.60 48.68% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 - TIT 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 35.09% ........... i.......... 130.... ' i 1 ' 1 1 1 1 m/z-- 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°-oxybis- 59 1 m 1 11.00 11.20 11.40 11.60 5000 31 45 m/ z 73.00 29.43% 103

134 m/z-> Abundance 20 ■ i • • ■ ■ i • ■ ■ ■ i • 1 ' ' i ' ' ■ ' I ' 30 40 50 60 70 ■ "II11/8/T . 80 90 100 । । 110 #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59 । । 120 । . k 130 । . 140

11.00 m/z TTT-r 11.20 41.00 0, U 11.40 A 1 I 1 1 1 1 I 11.60 24.36% 5000

m/z—> 20 31

30 |' 45 HI 1 ' I '■••T''' ' i 1 ' ' ' l ' 40 50 —.. 7.... .................. 60 70 80 90 100 110 120 130 140 TTT 11.00 TT■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 11.20 11.40 11.60

29930.D GCMS1126.M Fri Dec 28 13:29:10 2001 Page 2

NYC-WTC_000037037

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NYC-WTC_000037037Source: NYC Law Department, mirrored locally

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