GCMS analysis results for sample AD29930, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29930.D Vial: 8 Acq On : 15 Dec 2001 9:22 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.12 ug/1 817623 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl fori mide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxo] .ne, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 Pentane ,/3 - methoxy- 102 C6H140 036839-67-5 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 'Abundance Scan 278 (7.593 min): 29930.D (-) m/ z 73.00 100.00% 73

5000- 43 ITT — । । । । /1 । । 7.20 7.40 7.60 '.80 0( ------36 4 | 49 55 ... . 67,1 t......... 87............. 103.................... ’ I 1 ' ' ' I ' m/ Z 43.00 27.70% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

j 5000 58 7.20 7.40 7.60 7.80 8.00 44 m/ Z 41.00 10.50% 15 J ■ T....... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bro’no-5.5,5-trichloro-2,2-dimet 73 7.20 7.40 7.60 7.80 8.00 5000 - m/z 45.05 9.88% 45 36 55 67..................................... 109 115 1 • i 1 1 ■ ■ i ' ■ ■ ■ i • ■ ! ■ i 1 ■ ' ■ i ■ ' ■ ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1793: Pentane, 3-methoxy- —PP । /1 । । T-r-i-r-r-r-r-|-T-T 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.32% 5000- 45

........ 2733 39 I I I • I I I « I I ITICITT II 55 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29930.D GCMS1126.M Fri Dec 28 13:29:06 2001 Page 1

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