GCMS analysis results for sample AD29664, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29664.D Vial: 16 Acq On 15 Dec 2001 5:10 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.43 ug/1 795888 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 4 3-Pentanol, 3-methyl-______ 102 C6H140 000077-74-7 9 Abundance 5 Scan 278 (7.599 min): 29664.D (-) m/ z 73.0.0 100.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00 I i ■ ■ ■ ■ i ■ ■ ■ ■ i 38441 50i ' 55■ 1'।'I 1 1 67. ' ' I । |...........87............... 103 m/z 43.0.0 27.41% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/ z 44.9.5 10.48%

miz-> 4 10 20 30 40 50 60 I k 70 | kl« . । . . • . । . . . . ( . » . . । > 80 90 100 110 Abundance #845: Silane, tetramethyl- 73

7.20 7.40 7.60 7.80 8.00 5000 - m/z 41.00 10.14% 45 15 31 55 88 T-r-pn-rT-r . . . , ।. ■ • i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ i ■ ■ ■ ■ i ■ ■ 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- IT '' > T, , । । i । ' । ! ! ! i T 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.86% 5000 45

27 33 39 . ■ ■ i ' ‘ ■ ■ i ■ • ■ ‘ i ■ ' ' ' i ' ' r 55 —IT ' ' ' ' i 1 ' ‘ TT '"| > TT | ' —I . .... , , , TnuT TIr Ti—rmmmmmom m/z-> 10 20 30 40 ’ 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29664.D GCMS1126.M Fri Dec 28 13:08:12 2001 Page 1

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