GCMS analysis results for sample AD29788, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29788.D Vial: 18 Acq On : 15 Dec 2001 7:07 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.46 ug/1 803409 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 3 3 -Pentanol ,. 3-methyl- 102 C6H140 000077-74-7 9 4 1 -Butanamine , 3-methyl- 87 C5H13N 000107-85-7 7 Abundance Scan 279 (7.607 min): 29788.D (-) m/ z 73.00 100.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 8.00 381 L50 55, - 67—1 m/ z 43.00 28.22% m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 - 58 7.20 7.40 7.60 7.80 8.00 44 1 m/ z 41.0.0 11.31%

m/z-> 15 i ' ' ■ 10 ' i 20 J I... 4 30 40 1 ' I 1 1 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 —TTTmnmprrTrr 7.20 7.40 7.60 7.80 8.00 5000 - m/z 45.05 11.07%

45 i 15 53 59 i 88 i BIT ' ' ' pnn—n—mn——mn————mm—Rmm———m-m miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- I • ■ • ' I ■ r 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 7.05% 5000 55 27 45 87 I , i ' ' ' ' i ' ' ' ' i 39, 1 ■ 1 । ■ 1 ' ' । ' ' 1 ■ । ' 1 — - - m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29788.D GCMS1126.M Fri Dec 28 13:23:48 2001 Page 1

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