GCMS analysis data for sample AD29517, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\29466.D Vial: 12 Acq On : 13 Dec 2001 8:37 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 2.05 ug/1 763369 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1-Butanamine, 3-methyl- _____ 87 C5H13N 000107-85-7 7 'Abundance Scan 278 (7.594 min): 29466.D (-) m/z 73.00 100.00% ! 73

.5000 43

|.......... 87 ............. 103 , 7.20 7.40 7.60 7.80 8.00 38 I, I 50 55 67, I I 0-1T P p dIddnmmnpumm m/z 43.0.5 27.76% m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000- 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.95 9.98% 6 1 ' 14 ' i lm/z-> 1G 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- 73 TTBnnnnnm 1 ' I 1 r TITTIIrr 7.20 7.40 7.60 7.80 8.00 5000 m/ z 41.0.5 9.93% 55 87 27 33 45 ■ ' i ■ ■ ■ ■ i ' ■ ■ 1111 I ( i ' ' ■ 1 i ■ ' ' ' i | . — m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- —I -----IPPIP 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 • 6.13% 5000

45 15 , 53 59 । 88 ■ ' । •1 • ■ । ■ • • • । ■ ■ > > । I l'. , । .'.'. ■ i' । , . . . । .'! . . । 11 -TPTPPPm m/z-> 10 20 ' 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29466.D GCMS1126.M Fri Dec 21 13:10:43 2001 Page 1

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