GCMS analysis results for sample AD30354, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30354.D Vial: 6 Acq On : 27 Dec 2001 4:03 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.62 4.40 ug/1 1628990 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance Scan 280 (7.618 min): 30354.D (-) m/z 72.95 100.00% 73

5000 43 * ‘‘t ' • i ~। > 7.207.40 7.80 8.00 .1 50 55 .61 67. i . 87 ’l’1,k 1’’ It I I l ill I > < I I I It > r-t"| i । i j | j i s38 IQ3 t* 1 j । m/ z 43.0.5 31.42% 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/z 45.05 11.16% ; 15 ■ 1 ■ i 1 11 1 1 । 1 1 • ■ •r-r-T-r '1 11 > • r1 miz-> 10 20 30 40 I50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 73 r' 1 ■ ' 1 1 ' 1 i 1 1 ' ' I 1 1 i ■ • 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.0,5 11.01%

45 15 31 55 88 T > | i i t I J ! > > i | I I ! T I 4TT74 | I sly TT 1 ' i 1 ‘ • i ■ ‘ ■ i ■ ■ ■ ■ i ‘ ' 1 1 i • miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentene, 3-methoxy- -1T I i rmm 1’ . 110 i । । i । 73 7.20 7.40— 7.60 7.80 8.00 m/z 71.00 6.95% 5000 45

27 33 3,9 , 55 11*’I’4* l"‘ 1 1 । । i > 110—t miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30354.D GCMS1126.M Wed Jan 02 10:53:51 2002 Page 1

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