GCMS analysis comments for sample AD29517 re-analysis required, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0302\29517.D Vial: 17 Acq On 4 Jan 2002 2:10 am Operator: 209 GALOS Sample gems scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

11.20 2.0G ug/1 1004440 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(zxfnethoxy-1-methylet 148 C7H1603 020324-32-7 78 2 2-Butanol, 3,3-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propano 11- (2-methoxypropoxy) - 148 C7H16O3 013429-07-7 50 4 2 - Propanol, 1,1' - oxybi s-__________ 134 C6H14O3 000110-98-5 50 Abundance / Scan 670 (11.195 min): 29517.D (-) m/z 59.05 100 . 00% | f 59

5000

-52— TT 45

73

89 103

........ 130.... ... M 10.80 11.00 11.20 11.40 ■ ■ T1 • 11.60

miz-> 20__ 30 40 50 60 70 80 ■I ’ 1 1 1 1 ' 90 1 T 110 100 120 130 140 m/ z 45.05 51.10% 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methy!ethoxy)- 59 I 5000

31 45 73 103 TP 10.80 — --I- 11.00 m/z 103.05 V 11.20 ML 11.40 33.35% 11.60

—......... — ..... i........... 130..... PTTPT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 59 I ' ’ ' rI i 10.80 11.00 11.20 ' I 1 ’ 11.40 11.60 5000 - 31 45 m/ z 73.00 26.45% 103 I

. । i , n । , , .-r-p- .. ; .......... ! 134 m/z-> Abundance 20 30 40 50__ 60___ 70 80 90 100 110 #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59 120 130 140 —A 10.80 11.00 11.20 11.40 11.60 m/ z 41.05 24.78% 5000 -

31 45 V ' I 1 11 'I1 I -- 73 104 130 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 10.80 11.00 11.20 11.40 11.60

29517.D GCMS1126.M Tue Jan 08 12:19:38 2002 Page 4

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