GCMS comments for sample AD29520, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\1\DATA\JAN0302\29520 . D Vial: 16 Acq On 4 Jan 2002 1:12 am Operator: 209 GALOS Sample gems scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.27 2.89 ug/1 1599490 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 17(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 2-Propanol, X, 1 ‘ -oxybis- 134 C6H14O3 000110-98-5 50 3 1-Propanol, /2-(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 45 4 2-Butanol/ 3,3'-oxybis- 162 C8H18O3 054305-61-2 42 'Abundance Scan 678 (11.271 min): 29520.D (-) m/z 59.05 100.00% 59

5000- 45

—ll 53 4—6 TT70“t 67 73

85 91 103

■ i — । । । । । । । । 130 11.00 M 11.20 11.40 11.60 TIT ■ i ' ■ ■ ' i ' m/ z 45.00 52.08% miz-> 30 40 !50 60 80 90 100 110 120 130 140 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)-

5000

31 45 59

73 103 11.00 m/z 103.05 _VA 11.20 11.40 11.60 31.04% .... ...... ...... ............... 1 130 30___ 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087; 2-Propanol. 1,1’-oxybis- ’ 59 . ————— 31 11.00 11.20 1140 11.60 5000- 45 m/z 26.37% 73 • 00 103 I 89 ......... . 72 IIt ' i ' ' ' ' i ' ■ ' ' i ' ' ' ' i ' ■ miz-> 30 40 50 60 70 80 90 100 11 . 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy) . TI 59 11.00 11.20 11.40 11.60 m/z 41.0.5; 25.57% 5000 — 31 45 103

75 89 1i■■■'।11■ ....... ।।।»11।।. m/z-> 30 40 50 I60 70 80 90 100 110 120 130 140 11.1 11.20 11.40 11.60

29520.D GCMS1126.M Tue Jan 08 10:29:04 2002 Page 5

NYC-WTC_000036553