GCMS comments for sample AD29520, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0302\29520.D Vial: 16 Acq On 4 Jan 2002 1:12 am Operator: 209 GALOS Sample gems scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ****************************************** * * *** * ** * ************** * * * * Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.19 2.53 ug/1 1400050 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID' MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 2-Propanol, 1,1 -oxybis- 134 C6H14O3 000110-98-5 50 3 1-Propanol, 2 -2-hydroxypropoxy)- 134 C6H14O3 000106-62-7- 45 4 2-Propanol, 1- (2-methoxypropoxy)- 148 C7H16O3 013429-07-7 40 'Abundance Scan 669 (11.189 min): 29520.D (-) m/z 59.05 100.00% 59

5000

—al —53 4... 45

73

83 89 103

4 130 . M 10.80 11.00 11.20 11.40 m/z 45.05 51.88% 11.60 I TT+r miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 1 1 1 1 ' T —I 45 103 10.80 11.00 11.20 11.40 11.60 73 31 m/z 103.00. 29.73% — ........... ,.......... 130 —— — T m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol, 1,1‘-oxybis- - 59

10.80 11.00 11.20 11.40 11.60 31 5000 45 m/ z 73.00 26.15% 103

m/z-> Abundance . 72 ' i ■ ■ ' ' i ' ■ ' ■ I ■ ■ ' 1 i ■ ' ' ■ i ' 1 30 40 50 60 70 80 89

90 100 #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 110 120 130 . AL 10.80 m/ z 11.00 41.00 11.20 A 11.40 25.32% 11.60

N 5000 31 45 103

• • i ■ • ■ • । • II 75 89 1 1 i —+FT ■ । • ■ ■ ■ i 1 ■ ■ ■ i ' ' ■ ■ i ' ' ■ ■ i ■ ■ ■ ' i ' ■ ' • i ' 1 —P— JV m/z-> 30 40 50 I 60 70 80 90 100 110 120 130 10.80 11.00 11.20 11.40 11.60

29520.D GCMS1126.M Tue Jan 08 10:29:00 2002 Page 4

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