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GCMS analysis results for sample AD29667, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036815–000036830

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036824
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NYC 9/11 Public Portal Document

Library Search Compound Report

■ Data File C:\HPCHEM\1\DATA\DEC3101\29667.D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

11.36 0.31 ug/1 130664 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-metnoxy-l-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 50 3 2-Propanol, 1-(2< methoxypropoxy)- 148 C7H1603 013429-07-7 43 4 1-Propanol, 2 —2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 • Scan 688 (11.358 min): 29667.D (-) Abundance m/z.................................. 59.05■ 100.00% ■ 59

5000 - 45 73 103

A I 11.00 11.20 11.40 11.60 __ I

miz-s TIT 30 —ll 40 i* 1 । । i-1'I— 50 60 I " ' r1 + 70 80 88 90 100 1107 120 130 m/z 45.05, 48.84% Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

—----- I TT PPI 5000 103 45 11.00 11.20 11.40 11.60 _ 73 31 m/z 103.00/ 28.28% 130 miz-> PP40- —P30 50 Knnn 60 70 80 90 100 110 1120 130 Abundance #6087: 2-Propanol. 1,1-oxybis- 59 i TI = TT 31 11.00 11.20 11.40 11.60

M 5000- 45 m/z 73.00 27.58% 103 89 1 . 72 1 1 ' ' • ' 1 ' ' ■ ' i ' ■ • 1 1 1 ' ■ ■ 1 1 ' I ,

m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 11'20 59 11.00 11.40 11.60 m/z 41.05 24.48% 5000

31 45 73 104 ■ ■ J...... --- — mIPmm 130 1 • 1' miz-> 30 40 50 60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

29667.D GCMS1126.M Wed Jan 16 14:47:48 2002 Page 3

NYC-WTC_000036824

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NYC-WTC_000036824Source: NYC Law Department, mirrored locally

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