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GCMS analysis results for sample AD29667, Jan 2002

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GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036815–000036830

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036825
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NYC 9/11 Public Portal Document Library Search Compound Report

,Data File C:\HPCHEM\l\DATA\DEC3101\29667.D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-Propanol, 2-(2-hydroxypropox Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.34 ug/1 142437 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Propanol, 2- (2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 40 2 2-Propanol, 1,1-oxybis- 134 C6H14O3 000110-98-5 40 3 Ethane, 1,2- diethoxy- 118 C6H14O2 000629-14-1 36 4 Ether A 74 C4H10O 000060-29-7 36 Abundance • Scan 697 (11,441 min); 29667.D (-) m/z 59.05 100.00%

5000- 45 59

73 103 UN N 11.20 11.40 11.60 11.80 86 —4।— T i —PT T >. TI m/z 45.05 55.50% m/z-> 10 20 30 40 50 (60 70 80 90 100 110 120 'Abundance #6086; 1-Propanol, 2-(2-hydroxypropoxy)- 59

5000 ----------------- -I 31 11.20 11.40 11.60 11.80 45 103 m/ z 103.05 32.90% ----------------- # ' 75 89 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #6087; 2-Propanol, 1,1-oxybis- 59 T 11.20 11.40 11.60 11.80 31 5000- 45 I m/z 73.00 27.71% 103 89 , . 72 --d—nT/CEFE—-Tr-—1/TTT-T*1/r/"d/B.1 m/z--> 10 20 30 40 . 50 60 70 80 90 100 110 120 Abundance #3546: Ethane, 1,2-diethoxy- 31 11.20 11.40 11.60 11.80

MN 59 m/ z 41.05 25.29% 45 5000 74

15

m/z-> r-j-r-!-.I . । , , , >-p -- t 118 -— VVV 10 20 30 40 50 60 70 80 90 100 110 120 11.20 11.40 11.60 11.80

29667.D GCMS1126.M Wed Jan 16 14:47:52 2002 Page 4

NYC-WTC_000036825

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NYC-WTC_000036825Source: NYC Law Department, mirrored locally

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