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GCMS analysis results for sample AD29733, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29733 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037177–000037187

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29733.D Vial: 20 Acq On 15 Dec 2001 9:03 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.48 ug/1 127917 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-l-methylet 148 C7H16O3 020324-32-7 64 2 2-Propanol, I ZL ‘ -oxybis- 134 C6H14O3 000110-98-5 50 3 2-Propanol, 1-(2-methoxypropoxy) - 148 C7H16O3 013429-07-7 47 4 Ethane, l-e€hoxy-l-methoxy-_______ 104 C5H12O2 010471-14-4 47 Abundance Scan 696 (11.431 min): 29733.D (-) m/ z 59.05 100.00% 59

5000 45

73 • 103 _N N 11.20 11.40 11.60 11.80

m/z-> ■ ' i 30 —3ll +1) ■ 40 50 51 60 TH 70 .i , 80 90 100 + 110 87 120 130 m/z 45.00 49.62% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.20 11.40 11.60 11.80 73 31 m/ z 103.05 32.61% I , i ——— T — PPP 130 ' i ' IIT nn m/z—> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087; 2-Propanol, 1,1-oxybis- 59l TTT I T"" 11.20 11.40 11.60 11.80 31 5000 45 m/z 73.00 26.70%

—M 103 . । 89 I 72 • i • ■ • ■ । ■ ■ i ■ • • ■ i ■ ■ i ■ ' ' ■ i ■ ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)-

, NJ 59 11.20 11.40 11.60 11.80 m/z 41.00 23.38% 5000-

31 45 73 104 | —— -------------- 130 ■ ' i ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 11.20 11.40 11.60 11.80

29733.D GCMS1126.M Fri Dec 28 13:11:29 2001 Page 3

NYC-WTC_000037186

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