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GCMS analysis data for sample AD29466, Jan 2002

Machine-extracted title · confidence 95%

Raw GCMS analysis data and chromatogram details for sample AD29466 including surrogate recovery results.

NYC-WTC_000036603–000036613

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\29464.D Vial: 14 Acq On : 13 Dec 2001 10:34 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.41 1.93 ug/1 703995 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative7 ID MW MolForm CAS# Qual

l 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1- (2-methoxypropoxy) - 148 C7H1603 013429-07-7 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 694 (11.413 min): 29464.D (-) m/z 59.05 100. 00% 59

5000-

———— 45 73

85 । 103

130 ... M_ 11.00 11.20 11.40 11.60 11.80 -4— ' ■ ' 14 m/z 44.95 48.95%

A m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000- 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103 .05 34.54% ..... - 130 ' I ' ' ' 1 I ' ' ' ' 1 1 1 ' ' I ' ' ttgrnn ! | I ■ I I I | I I I I | I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3‘-oxybis- 59 1 I 1 1 11.00 11.20 11.40 11.60 11.80 5000- 31 45 m/z 73.00 28.14% 103

m/z-> Abundance 20 I . 30 | 40 I ' | 50 1. ____________________________ ( i i . . I . r, । । । . । । ! । < । . ! । ■ i r J r I i 1 | | i 60 70 80 90 #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59 100 110 120 130 140 134 ' ' i ' ' ' ' i '

m/z NA 11.00 11.20 11.40 11.60 11.80 41.05 24.40%

111. 5000

31 45

m/z-> I Ui | 11 11 ■■I'■■■।■■■’।■ 20 30 40 50 — 60 l........... 70 80 90 194 ... —130 .... 100 110 120 130 140 11.00 11.20 11.40 11.60 80

29464.D GCMS1126.M Fri Dec 21 13:09:44 2001 Page 3

NYC-WTC_000036612

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NYC-WTC_000036612Source: NYC Law Department, mirrored locally

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